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Synthesis of a new iron (III) porphyrin acrylate-styrene copolymer and its catalysis for hydroxylation of cyclohexane

YU Hancheng, LI Xixian, HUANG Jinwang, JI Liangnian, CHEN Xianli

《化学科学与工程前沿（英文）》 2007年 第1卷 第1期   页码 65-67 doi: 10.1007/s11705-007-0013-9

摘要： A new iron (III) porphyrin acrylate-styrene copolymer, P[(PorFe)A-S], was synthesized by the reaction of iron (III) porphyrin acrylate with styrene and characterized by UV-Vis, Infrared spectra (IR), inductively coupled plasma-atomic emission spectrometry (ICP) and molecular weight determination. Its catalytic activity in the hydroxylation of cyclohexane for model cytochrome P450 in the P[(PorFe)A-S]-O ascrobate-thiosalicylic acid system has been studied. It was found that the P[(PorFe)A-S] has a higher catalytic activity than non-supported iron (III) porphyrin and its high catalytic activity remained in reuse. The catalytic activity of P[(PorFe)A-S] was discussed in the view of the microenvironment of iron (III) porphyrin. It is proposed that the atalytic activity of the P[(PorFe)A-S] may be further enhanced by construction of a homophase catalytic system containing the iron (III) porphyrin acrylate-styrene copolymer.

关键词： plasma-atomic emission     UV-Vis     weight determination     acrylate-styrene copolymer     styrene    

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Solving topology optimization problems by the Guide-Weight method

Xinjun LIU, Zhidong LI, Liping WANG, Jinsong WANG

《机械工程前沿（英文）》 2011年 第6卷 第1期   页码 136-150 doi: 10.1007/s11465-010-0126-6

摘要：

Finding a good solution method for topology optimization problems is always paid attention to by the research field because they are subject to the large number of the design variables and to the complexity that occurs because the objective and constraint functions are usually implicit with respect to design variables. Guide-Weight method, proposed first by Chen in 1980s, was effectively and successfully used in antenna structures’ optimization. This paper makes some improvement to it so that it possesses the characteristics of both the optimality criteria methods and the mathematical programming methods. When the Guide-Weight method is applied into topology optimization, it works very well with unified and simple form, wide availability and fast convergence. The algorithm of the Guide-Weight method and the improvement on it are described; two formulations of topology optimization solved by the Guide-Weight method combining with SIMP method are presented; subsequently, three numerical examples are provided, and comparison of the Guide-Weight method with other methods is made.

关键词： Guide-Weight method     topology optimization     SIMP method    

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Progress in studies of sex determination mechanisms and sex control techniques in

Qian ZHOU,Songlin CHEN

《农业科学与工程前沿（英文）》 2016年 第3卷 第2期   页码 113-123 doi: 10.15302/J-FASE-2016093

摘要： The (half-smooth tongue sole) is a marine flatfish of great commercial value for fisheries and aquaculture in China. It has a female heterogametic sex determination system (ZW/ZZ) and environmental factors can induce sex-reversal of females to phenotypic males, suggesting that it is a promising model for the study of sex determination mechanisms. Additionally, females grow much faster than males and it is feasible to improve the aquaculture production through sex control techniques. This paper reviews the progress in research on sex determination mechanisms research in our laboratory. We have completed whole-genome sequencing and revealed the genome organization and sex chromosome evolution of . A putative male determining gene was identified and DNA methylation was verified as having a crucial role in the sex reversal process. Genetic maps and sex-specific biomarkers have been used in a marker-assisted selection breeding program and for differentiation of the fish sex. Development and improvement of sex control technologies, including artificial gynogenesis and production of breeding fry with high proportion of females, is also reviewed. These research advances have provided insight into the regulation of sex determination and enabled efficient sex management in artificial culturing of .

关键词： Cynoglossus semilaevis     sex determination     sex control technique    

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Instantaneous deflection of light-weight concrete slabs

Behnam VAKHSHOURI, Shami NEJADI

《结构与土木工程前沿（英文）》 2017年 第11卷 第4期   页码 412-423 doi: 10.1007/s11709-017-0416-8

摘要： Construction loading before the age of 28 d can have the most significant effects on the slabs, especially for multi-story structures. The changing properties of the young concrete complicate the prediction of serviceability design requirements also. An experimental investigation is performed on four simply supported Light-Weight Concrete (LWC) one-way slabs subjected to immediate loading at 14 d. Effects of aggregate type, loading levels and cracking moment together with the influences of ultimate moment capacity and service moment on the instantaneous deflection of slabs are studied. Comparison of the obtained results with predictions of existing models in the literature shows considerable differences between the recorded and estimated instantaneous deflection of LWC slabs. Based on sensitivity analysis of the effective parameters, a new equation is proposed and verified to predict the instantaneous deflection of LWC slabs subjected to loading at the age of 14 d.

关键词： instantaneous deflection     light-weight concrete     expanded polystyrene     effective moment of inertia     cracking moment     moment capacity     service moment    

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Characterization of soil low-molecular-weight organic acids in the Karst rocky desertification region

Xiaoliang LI, Xiaomin CHEN, Xia LIU, Lianchuan ZHOU, Xinqiang YANG

《环境科学与工程前沿（英文）》 2012年 第6卷 第2期   页码 195-203 doi: 10.1007/s11783-012-0391-1

摘要： Soil low-molecular-weight (LMW) organic acids play important roles in the soil-forming process and the cycling of nutrients in Karst regions. In this study, we quantified the contents of LMW organic acids (including lactate, acetate, formate, malate, and oxalate) in soil solution over the Karst region of Guizhou Province, China using ion chromatography. The concentration of total LMW organic acids in topsoil solution ranged from 0.358 to 1.823 μmol·g , with an average of 0.912 μmol·g . The mean concentrations of lactate, acetate, formate, malate, and oxalate were 0.212±0.089, 0.302±0.228, 0.301±0.214, 0.014±0.018 and 0.086±0.118 μmol·g , respectively. There were also significant difference in the contents of these acids among four phases of rocky desertification, and their concentrations decreased with the aggravation of rocky desertification. The concentrations of the LMW organic acids were significantly positive correlated each other. Significant positive correlations were also observed among individual LMW organic acids in soil solution, and between them and soil available P, available K, exchangeable Ca, respectively. Furthermore, the concentrations of LMW organic acids were significantly positively correlated with inorganic anions (chlorides, nitrates, and sulfates) in Karst topsoil solution. Therefore, the concentrations of soil LMW organic acids might be one of driving force in the Karst rock desertification process in Guizhou Province.

关键词： Karst rocky desertification     low-molecular-weight (LMW) organic acids     distribution characteristics     soil    

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Rapid method for on-site determination of phenolic contaminants in water using a disposable biosensor

Yuanting LI, Dawei LI, Wei SONG, Meng LI, Jie ZOU, Yitao LONG

《环境科学与工程前沿（英文）》 2012年 第6卷 第6期   页码 831-838 doi: 10.1007/s11783-012-0393-z

摘要： A disposable biosensor was fabricated using single-walled carbon nanotubes, gold nanoparticles and tyrosinase (SWCNTs-AuNPs-Tyr) modified screen-printed electrodes. The prepared biosensor was applied to the rapid determination of phenolic contaminants within 15 minutes. The SWCNTs-AuNPs-Tyr bionanocomposite sensing layer was characterized with scanning electron microscopy, electrochemical impedance spectroscopy and cyclic voltammetry methods. The characterization results revealed that SWCNTs could lead to a high loading of tyrosinase (Tyr) with the large surface area and the porous morphology, while AuNPs could retain the bioactivity of Tyr and enhance the sensitivity. The detection conditions, including working potential, pH of supporting electrolyte and the amount of Tyr were optimumed. As an example, the biosensor for catechol determination displayed a linear range of 8.0 × 10 to 2.0 × 10 mol·L with a detection limit of 4.5 × 10 mol·L (S/ = 3). This method has a rapid response time within 10 s, and shows excellent repeatability and stability. Moreover, the resulting biosensor could be disposable, low-cost, reliable and easy to carry. This kind of new Tyr biosensor provides great potential for rapid, on-site and cost-effective analysis of phenolic contaminants in environmental water samples.

关键词： on-site determination     tyrosinase biosensor     phenolic contaminants     single-walled carbon nanotubes     gold nanoparticles     screen-printed electrodes    

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Winner determination problem with loss-averse buyers in reverse auctions

Xiaohu QIAN, Min HUANG, Yangyang YU, Xingwei WANG

《工程管理前沿（英文）》 2017年 第4卷 第2期   页码 212-220 doi: 10.15302/J-FEM-2017019

摘要： Reverse auctions have been widely adopted for purchasing goods and services. This paper considers a novel winner determination problem in a multiple-object reverse auction in which the buyer involves loss-averse behavior due to uncertain attributes. A corresponding winner determination model based on cumulative prospect theory is proposed. Due to the NP-hard characteristic, a loaded route strategy is proposed to ensure the feasibility of the model. Then, an improved ant colony algorithm that consists of a dynamic transition strategy and a Max-Min pheromone strategy is designed. Numerical experiments are conducted to illustrate the effectiveness of the proposed model and algorithm. We find that under the loaded route strategy, the improved ant colony algorithm performs better than the basic ant colony algorithm. In addition, the proposed model can effectively characterize the buyer’s loss-averse behavior.

关键词： reverse auction     loss aversion     winner determination     improved ant colony algorithm    

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Prediction of falling weight deflectometer parameters using hybrid model of genetic algorithm and adaptive

《结构与土木工程前沿（英文）》   页码 812-826 doi: 10.1007/s11709-023-0940-7

摘要： A falling weight deflectometer is a testing device used in civil engineering to measure and evaluate the physical properties of pavements, such as the modulus of the subgrade reaction (Y1) and the elastic modulus of the slab (Y2), which are crucial for assessing the structural strength of pavements. In this study, we developed a novel hybrid artificial intelligence model, i.e., a genetic algorithm (GA)-optimized adaptive neuro-fuzzy inference system (ANFIS-GA), to predict Y1 and Y2 based on easily determined 13 parameters of rigid pavements. The performance of the novel ANFIS-GA model was compared to that of other benchmark models, namely logistic regression (LR) and radial basis function regression (RBFR) algorithms. These models were validated using standard statistical measures, namely, the coefficient of correlation (R), mean absolute error (MAE), and root mean square error (RMSE). The results indicated that the ANFIS-GA model was the best at predicting Y1 (R = 0.945) and Y2 (R = 0.887) compared to the LR and RBFR models. Therefore, the ANFIS-GA model can be used to accurately predict Y1 and Y2 based on easily measured parameters for the appropriate and rapid assessment of the quality and strength of pavements.

关键词： falling weight deflectometer     modulus of subgrade reaction     elastic modulus     metaheuristic algorithms    

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Comments on “Determination of heterozygosity for avirulence/virulence loci through sexual hybridization

Ralf T. Voegele

《农业科学与工程前沿（英文）》 2017年 第4卷 第1期   页码 121-122 doi: 10.15302/J-FASE-2017142

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Experimental determination of Cd

Farhah Amalya ISMAIL, Ahmad Zaharin ARIS

《环境科学与工程前沿（英文）》 2013年 第7卷 第3期   页码 356-364 doi: 10.1007/s11783-013-0488-1

摘要： Carbonate shells have an astonishing ability in the removal of Cd in a short time period with emphasis on being a low cost adsorbent. In the present study, the sorption capacity of carbonate shells was studied for Cd in batch experiments. The influence of different carbonate shell sizes and physico-chemical factors were evaluated and the results were analyzed for its correlation matrices by using Predictive Analytics Software (PASW). The mineralogy state of aqueous solution regarding the saturation index was simulated using PHREEQC to identify the Cd uptake mechanism. The Cd uptake rates were calculated as well as Ca , concentration, pH, ambient humidity and temperature were measured. Cd removal of 91.52% was achieved after 5 h adsorption. The adsorption efficiencies were significantly influenced by pH as they increased with the increase of pH from acidic solution (5.50±0.02) to slightly alkaline (7.60±0.05). In addition, the mineralogy state of aqueous solution calculated from PHREEQC confirmed that the increment of Ca and concentrations in solution was attributed to the dissolution of carbonate shells. Moreover, the ion exchange adsorption mechanism of Cd toward Ca was identified as the process involved in Cd uptake.

关键词： carbonate shell     cadmium     heavy metal     adsorption mechanism     saturation state    

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A simplified method for the determination of vertically loaded pile-soil interface parameters in layered

Jiu-jiang WU,Yan LI,Qian-gong CHENG,Hua WEN,Xin LIANG

《结构与土木工程前沿（英文）》 2016年 第10卷 第1期   页码 103-111 doi: 10.1007/s11709-015-0328-4

摘要： The numerical analysis of pile-soil interaction commonly requires a lot of trial works to determine the interface parameters and the accuracy cannot be ensured normally. Considering this, this paper first conducts a sensitivity analysis to figure out the influence of interface parameters on the bearing behavior of a single pile in sand. Then, a simplified method for the determination of pile-soil interface parameters in layered soil is proposed based on the parameter studies. Finally, a filed loading test is used for the validation of the simplified method, and the calculated results agree well with the monitoring data. In general, the simplified method proposed in this paper works with higher accuracy and consumes less time compared with the traditional trial works, especially on the determinations of interfacial cohesive and interfacial friction angle.

关键词： determination of interface parameters     pile-soil interaction     FLAC3D     sensitivity analysis     layered soil    

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Erratum to: Optimized determination of airborne tetracycline resistance genes in laboratory atmosphere

Lu Song, Can Wang, Yizhu Wang

《环境科学与工程前沿（英文）》 2020年 第14卷 第6期 doi: 10.1007/s11783-020-1289-y

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Build orientation determination of multi-feature mechanical parts in selective laser melting via multi-objective

《机械工程前沿（英文）》 2023年 第18卷 第2期 doi: 10.1007/s11465-022-0737-8

摘要： Selective laser melting (SLM) is a unique additive manufacturing (AM) category that can be used to manufacture mechanical parts. It has been widely used in aerospace and automotive using metal or alloy powder. The build orientation is crucial in AM because it affects the as-built part, including its part accuracy, surface roughness, support structure, and build time and cost. A mechanical part is usually composed of multiple surface features. The surface features carry the production and design knowledge, which can be utilized in SLM fabrication. This study proposes a method to determine the build orientation of multi-feature mechanical parts (MFMPs) in SLM. First, the surface features of an MFMP are recognized and grouped for formulating the particular optimization objectives. Second, the estimation models of involved optimization objectives are established, and a set of alternative build orientations (ABOs) is further obtained by many-objective optimization. Lastly, a multi-objective decision making method integrated by the technique for order of preference by similarity to the ideal solution and cosine similarity measure is presented to select an optimal build orientation from those ABOs. The weights of the feature groups and considered objectives are achieved by a fuzzy analytical hierarchy process. Two case studies are reported to validate the proposed method with numerical results, and the effectiveness comparison is presented. Physical manufacturing is conducted to prove the performance of the proposed method. The measured average sampling surface roughness of the most crucial feature of the bracket in the original orientation and the orientations obtained by the weighted sum model and the proposed method are 15.82, 10.84, and 10.62 μm, respectively. The numerical and physical validation results demonstrate that the proposed method is desirable to determine the build orientations of MFMPs with competitive results in SLM.

关键词： selective laser melting (SLM)     build orientation determination     multi-feature mechanical part (MFMP)     fuzzy analytical hierarchy process     multi-objective decision making (MODM)    

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Evaluation of ICUs and weight of quality control indicators: an exploratory study based on Chinese ICU

《医学前沿（英文）》 2023年 第17卷 第4期   页码 675-684 doi: 10.1007/s11684-022-0970-x

摘要： This study aimed to explore key quality control factors that affected the prognosis of intensive care unit (ICU) patients in Chinese mainland over six years (2015−2020). The data for this study were from 31 provincial and municipal hospitals (3425 hospital ICUs) and included 2 110 685 ICU patients, for a total of 27 607 376 ICU hospitalization days. We found that 15 initially established quality control indicators were good predictors of patient prognosis, including percentage of ICU patients out of all inpatients (%), percentage of ICU bed occupancy of total inpatient bed occupancy (%), percentage of all ICU inpatients with an APACHE II score ≥15 (%), three-hour (surviving sepsis campaign) SSC bundle compliance (%), six-hour SSC bundle compliance (%), rate of microbe detection before antibiotics (%), percentage of drug deep venous thrombosis (DVT) prophylaxis (%), percentage of unplanned endotracheal extubations (%), percentage of patients reintubated within 48 hours (%), unplanned transfers to the ICU (%), 48-h ICU readmission rate (%), ventilator associated pneumonia (VAP) (per 1000 ventilator days), catheter related blood stream infection (CRBSI) (per 1000 catheter days), catheter-associated urinary tract infections (CAUTI) (per 1000 catheter days), in-hospital mortality (%). When exploratory factor analysis was applied, the 15 indicators were divided into 6 core elements that varied in weight regarding quality evaluation: nosocomial infection management (21.35%), compliance with the Surviving Sepsis Campaign guidelines (17.97%), ICU resources (17.46%), airway management (15.53%), prevention of deep-vein thrombosis (14.07%), and severity of patient condition (13.61%). Based on the different weights of the core elements associated with the 15 indicators, we developed an integrated quality scoring system defined as F score=21.35%×nosocomial infection management + 17.97%×compliance with SSC guidelines + 17.46%×ICU resources + 15.53%×airway management + 14.07%×DVT prevention + 13.61%×severity of patient condition. This evidence-based quality scoring system will help in assessing the key elements of quality management and establish a foundation for further optimization of the quality control indicator system.

关键词： critical care medicine     quality control     evaluation     exploratory factor analysis (EFA) model    

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Uncovering the effect of poly(ethylene-co-vinyl alcohol) molecular weight and vinyl alcohol content on

《化学科学与工程前沿（英文）》 2023年 第17卷 第10期   页码 1484-1502 doi: 10.1007/s11705-023-2331-y

摘要： Various hydrophilic poly(ethylene-co-vinyl alcohol) (EVOH) were used herein to precisely control the structure and hydrodynamic properties of polysulfone (PSF) membranes. Particularly, to prepare pristine PSF and PSF/EVOH blends with increasing vinyl alcohol (VOH: 73%, 68%, 56%), the non-solvent-induced phase separation (NIPS) technique was used. Polyethylene glycol was used as a compatibilizer and as a porogen in N,N-dimethylacetamide. Rheological and ultrasonic separation kinetic measurements were also carried out to develop an ultrafiltration membrane mechanism. The extracted membrane properties and filtration capabilities were systematically compared to the proposed mechanism. Accordingly, the addition of EVOH led to an increase in the rheology of the dopes. The resulting membranes exhibited a microporous structure, while the finger-like structures became more evident with increasing VOH content. The PSF/EVOH behavior was changed from immediate to delayed segregation due to a change in the hydrodynamic kinetics. Interestingly, the PSF/EVOH32 membranes showed high hydrophilicity and achieved a pure water permeability of 264 L·m–2·h–1·bar–1, which was higher than that of pure PSF membranes (171 L·m–2·h–1·bar–1). In addition, PSF/EVOH32 rejected bovine serum albumin at a high rate (> 90%) and achieved a significant restoration of permeability. Finally, from the thermodynamic and hydrodynamic results, valuable insights into the selection of hydrophilic copolymers were provided to tailor the membrane structure while improving both the permeability and antifouling performance.

关键词： polysulfone     blend modification     ultrafiltration membrane     formation hydrodynamics     poly(ethylene-co-vinyl alcohol) copolymer    

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标题 作者 时间 类型 操作

Synthesis of a new iron (III) porphyrin acrylate-styrene copolymer and its catalysis for hydroxylation of cyclohexane

YU Hancheng, LI Xixian, HUANG Jinwang, JI Liangnian, CHEN Xianli

期刊论文

Solving topology optimization problems by the Guide-Weight method

Xinjun LIU, Zhidong LI, Liping WANG, Jinsong WANG

期刊论文

Progress in studies of sex determination mechanisms and sex control techniques in

Qian ZHOU,Songlin CHEN

期刊论文

Instantaneous deflection of light-weight concrete slabs

Behnam VAKHSHOURI, Shami NEJADI

期刊论文

Characterization of soil low-molecular-weight organic acids in the Karst rocky desertification region

Xiaoliang LI, Xiaomin CHEN, Xia LIU, Lianchuan ZHOU, Xinqiang YANG

期刊论文

Rapid method for on-site determination of phenolic contaminants in water using a disposable biosensor

Yuanting LI, Dawei LI, Wei SONG, Meng LI, Jie ZOU, Yitao LONG

期刊论文

Winner determination problem with loss-averse buyers in reverse auctions

Xiaohu QIAN, Min HUANG, Yangyang YU, Xingwei WANG

期刊论文

Prediction of falling weight deflectometer parameters using hybrid model of genetic algorithm and adaptive

期刊论文

Comments on “Determination of heterozygosity for avirulence/virulence loci through sexual hybridization

Ralf T. Voegele

期刊论文

Experimental determination of Cd

Farhah Amalya ISMAIL, Ahmad Zaharin ARIS

期刊论文

A simplified method for the determination of vertically loaded pile-soil interface parameters in layered

Jiu-jiang WU,Yan LI,Qian-gong CHENG,Hua WEN,Xin LIANG

期刊论文

Erratum to: Optimized determination of airborne tetracycline resistance genes in laboratory atmosphere

Lu Song, Can Wang, Yizhu Wang

期刊论文

Build orientation determination of multi-feature mechanical parts in selective laser melting via multi-objective

期刊论文

Evaluation of ICUs and weight of quality control indicators: an exploratory study based on Chinese ICU

期刊论文

Uncovering the effect of poly(ethylene-co-vinyl alcohol) molecular weight and vinyl alcohol content on

期刊论文